农药(第1卷)/农药兽药多组分残留质谱分析技术

本书特色

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本书是《农药兽药多组分残留质谱分析技术》的第1卷农药篇，介绍了农药多残留分析技术和千余种农药不同色谱-质谱条件下的质谱参数，实现了一次样品制备，GC-MS和LC-MS/MS同时测定，扩大了检测目标的范围。书中包括20项适用于10余类农产品（包括水果、蔬菜、粮谷、茶叶、中草药、食用菌、果蔬汁、蜂蜜、动物组织、水产品、牛奶、奶粉及饮用水）中800多种农药化学污染物残留的色谱-质谱分析方法。

本书可供从事食品安全、农业环境保护及农药开发利用等技术研究与应用的技术人员参考，也可作为大学教学参考用书。

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内容简介

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本书是《农药兽药多组分残留质谱分析技术》的卷农药篇，介绍了农药多残留分析技术和千余种农药不同色谱-质谱条件下的质谱参数，实现了一次样品制备，GC-MS和LC-MS/MS同时测定，扩大了检测目标的范围。书中包括20项适用于10余类农产品（包括水果、蔬菜、粮谷、茶叶、中草药、食用菌、果蔬汁、蜂蜜、动物组织、水产品、牛奶、奶粉及饮用水）中800多种农药化学污染物残留的色谱-质谱分析方法。
本书可供从事食品安全、农业环境保护及农药开发利用等技术研究与应用的技术人员参考，也可作为大学教学参考用书。

]

作者简介

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庞国芳，中国检验检疫科学研究院，研究员，中国工程院院士，国家质检总局首席研究员、国际公职化学家联合会（AOAC）专家，国际AOAC 2014年度 Harvey W. Wiley 奖获得者。近30年一直工作在食品检验检疫一线，致力于食品科学检测技术理论与实践的研究，解决了我国相关出口食品、农产品等遭遇的技术瓶颈，为推动我国对外贸易发展做出了杰出贡献。研究制定了141项国际、国家检测技术标准。在国内、国际出版食品安全检测技术论著10部。发表论文100余篇，35篇被SCI收录。3次荣获国家科学技术进步二等奖，6次荣获国际AOAC组织颁发的科学技术奖励。

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目录

Main Researchers/Editors xiiiPreface xvBrief Introduction xvii1. Introduction 11.1 Insecticides 11.1.1 Organophosphate Insecticides 11.1.2 Carbamate Insecticides 21.1.3 Organochlorine Insecticides 21.1.4 Pyrethroid Insecticides 21.1.5 Neonicotinoid Insecticides 21.2 Herbicides 31.2.1 Phenolic Herbicides 31.2.2 Phenoxy Acid Herbicides 31.2.3 Benzoic Acid Herbicides 41.2.4 Diphenyl Ether Herbicides 41.2.5 Dinitroaniline Herbicides 41.2.6 Amide Herbicides 41.2.7 Carbamate Herbicides 51.2.8 Thiocarbamate Herbicides 51.2.9 Urea Herbicides 51.2.10 Sulfonylurea Herbicides 51.2.11 S-Triazine Herbicides 51.2.12 Quaternary Ammoniums Herbicides 61.2.13 Organophosphate Herbicides 61.2.14 Other Herbicides 61.3 Bactericides 61.3.1 Triazole Bactericides 71.3.2 Amide Bactericides 71.3.3 Pyridinamine Bactericides 71.3.4 Strobin Bactericides 71.3.5 Oxazo Bactericides 81.3.6 Pyrrole Bactericides 81.3.7 Amino Acid Bactericides 81.3.8 Derivants of Cinnamic Acid 81.3.9 Others 81.4 Pesticides Banned in the World 81.4.1 Pesticides Banned in China 81.4.2 Pesticides Banned in Japan 91.4.3 Pesticides Banned in European Union 92. Analytical Methods for 793 Pesticides and RelatedChemical Residues in Products of Plant Origin 112.1 Determination of 512 Pesticides and Related Chemical Residuesin Fruit Juice and Wine: LC-MS-MS Method (GB/T 23206-2008) 112.1.1 Scope 112.1.2 Principle 112.1.3 Reagents and Materials 112.1.4 Apparatus 212.1.5 Sample Pretreatment 212.1.6 Determination 222.1.7 Precision 24Researchers 242.2 Determination of 500 Pesticides and Related Chemical Residuesin Fruits and Vegetables: GC-MS Method (GB/T 19648-2006) 252.2.1 Scope 252.2.2 Principle 252.2.3 Reagents and Materials 252.2.4 Apparatus 352.2.5 Sample Pretreatment 352.2.6 GC-MS Determination 362.2.7 Precision 37Researchers 372.3 Determination of 450 Pesticides and Related Chemical Residuesin Fruits and Vegetables: LC-MS-MS Method(GB/T 20769-2008) 372.3.1 Scope 372.3.2 Principle 452.3.3 Reagents and Materials 452.3.4 Apparatus 462.3.5 Sample Pretreatment 462.3.6 Determination 472.3.7 Precision 49Researchers 502.4 Determination of 475 Pesticides and Related Chemical Residuesin Grains: GC-MS Method (GB/T 19649-2006) 502.4.1 Scope 502.4.2 Principle 502.4.3 Reagents and Materials 502.4.4 Apparatus 592.4.5 Sample Pretreatment 592.4.6 GC-MS Method Determination 602.4.7 Precision 61Researchers 612.5 Determination of 486 Pesticides and Related Chemical Residuesin Grains: LC-MS-MS Method (GB/T 20770-2008) 612.5.1 Scope 612.5.2 Principle 692.5.3 Reagents and Materials 692.5.4 Apparatus 712.5.5 Sample Pretreatment 712.5.6 Determination 722.5.7 Precision 73Researchers 732.6 Determination of 519 Pesticides and Related ChemicalResidues in Tea Leaves: GC-MS Method (GB/T 23204-2008) 742.6.1 Scope 742.6.2 Determination of 490 Pesticides and Related Chemical Residues in Tea: GC-MS Method 742.6.3 Determination of 29 Acidic Herbicides in Tea:GC-MS Method 85Researchers 912.7 Determination of 448 Pesticides and Related ChemicalResidues in Tea Leaves: LC-MS-MS Method (GB/T23205-2008) 922.7.1 Scope 922.7.2 Principle 922.7.3 Reagents and Materials 922.7.4 Apparatus 1012.7.5 Sample Pretreatment 1012.7.6 Determination 1022.7.7 Precision 103Researchers 1032.8 Determination of 488 Pesticides and Related ChemicalResidues in Mulberry Twig, Honeysuckle, Barbary WolfberryFruit, and Lotus Leaf: GC-MS Method (GB/T 23200-2008) 1032.8.1 Scope 1032.8.2 Principle 1042.8.3 Reagents and Materials 1042.8.4 Apparatus 1132.8.5 Sample Pretreatment 1132.8.6 Determination 1142.8.7 Precision 115Researchers 1152.9 Determination of 413 Pesticides and Related ChemicalResidues in Mulberry Twig, Honeysuckle, Barbary WolfberryFruit, and Lotus Leaf: LC-MS-MS Method (GB/T 23201-2008) 1152.9.1 Scope 1152.9.2 Principle 1152.9.3 Reagents and Materials 1162.9.4 Apparatus 1232.9.5 Sample Pretreatment 1232.9.6 Determination 1242.9.7 Precision 126Researchers 1262.10 Determination of 503 Pesticides and Related ChemicalResidues in Mushrooms: GC-MS Method (GB/T 23216-2008) 1262.10.1 Scope 1262.10.2 Principle 1262.10.3 Reagents and Materials 1272.10.4 Apparatus 1362.10.5 Sample Pretreatment 1362.10.6 Determination 1372.10.7 Precision 138Researchers 1382.11 Determination of 440 Pesticides and Related ChemicalResidues in Edible Fungus: LC-MS-MS Method(GB/T 23202-2008) 1382.11.1 Scope 1382.11.2 Principle 1382.11.3 Reagents and Materials 1462.11.4 Apparatus 1472.11.5 Sample Pretreatment 1472.11.6 Determination 1482.11.7 Precision 149Researchers 1493. Analytical Methods for 790 Pesticides and RelatedChemical Residues in Products of Animal Origin 1513.1 Determination of 511 Pesticides and Related ChemicalResidues in Milk and Milk Powder: GC-MS Method(GB/T 23210-2008) 1513.1.1 Scope 1513.1.2 Principle 1513.1.3 Reagents and Materials 1513.1.4 Apparatus 1623.1.5 Sample Pretreatment 1623.1.6 Determination 1633.1.7 Precision 164Researchers 1643.2 Determination of 493 Pesticides and Related ChemicalResidues in Milk and Milk Powder: LC-MS-MS Method(GB/T 23211-2008) 1653.2.1 Scope 1653.2.2 Principle 1653.2.3 Reagents and Materials 1653.2.4 Apparatus 1753.2.5 Sample Pretreatment 1753.2.6 Determination 1763.2.7 Precision 178Researchers 1783.3 Determination of 485 Pesticides and Related ChemicalResidues in Fugu, Eel, and Prawn: GC-MS Method(GB/T 23207-2008) 1793.3.1 Scope 1793.3.2 Principle 1873.3.3 Reagents and Materials 1873.3.4 Apparatus 1883.3.5 Sample Pretreatment 1893.3.6 Determination 1903.3.7 Precision 191Researchers 1913.4 Determination of 450 Pesticides and Related ChemicalResidues in Fugu, Eel, and Prawn: LC-MS-MS Method(GB/T 23208-2008) 1923.4.1 Scope 1923.4.2 Principle 2003.4.3 Reagents and Materials 2003.4.4 Apparatus 2013.4.5 Sample Pretreatment 2013.4.6 Determination 2033.4.7 Precision 204Researchers 2043.5 Determination of 497 Pesticides and Related ChemicalResidues in Honey, Fruit Juice, and Wine: GC-MS Method(GB/T 19426-2006) 2043.5.1 Scope 2043.5.2 Principle 2043.5.3 Reagents and Materials 2133.5.4 Apparatus 2143.5.5 Sample Pretreatment 2143.5.6 Determination 2153.5.7 Precision 216Researchers 2173.6 Determination of 486 Pesticides and Related ChemicalResidues in Honey: LC-MS-MS Method (GB/T 20771-2008) 2173.6.1 Scope 2173.6.2 Principle 2173.6.3 Reagents and Materials 2173.6.4 Apparatus 2273.6.5 Sample Pretreatment 2273.6.6 Determination 2283.6.7 Precision 232Researchers 2323.7 Determination of 478 Pesticides and Related ChemicalResidues in Animal Muscles: GC-MS Method(GB/T 19650-2006) 2323.7.1 Scope 2323.7.2 Principle 2323.7.3 Reagents and Materials 2323.7.4 Apparatus 2423.7.5 Sample Pretreatment 2423.7.6 Determination 2433.7.7 Precision 244Researchers 2443.8 Determination of 461 Pesticides and Related ChemicalResidues in Animal Muscles: LC-MS-MS Method(GB/T 20772-2008) 2453.8.1 Scope 2453.8.2 Principle 2533.8.3 Reagents and Materials 2533.8.4 Apparatus 2543.8.5 Sample Pretreatment 2543.8.6 Determination 2563.8.7 Precision 257Researchers 2574. Determination of 450 Pesticides and RelatedChemical Residues in Drinking Water: LC-MS-MS Method (GB/T 23214-2008) 2594.1 Scope 2594.2 Principle 2594.3 Reagents and Materials 2594.4 Apparatus 2684.5 Sample Pretreatment 2694.5.1 Preparation of Test Sample 2694.5.2 Extraction 2694.5.3 Clean-up 2694.6 Determination 2694.6.1 LC-MS-MS Operating Condition 2694.6.2 Qualitative Determination 2714.6.3 Quantitative Determination 2714.7 Precision 272Researchers 2725. Basic Research on Chromatography-Mass SpectroscopyCharacteristic Parameters of Pesticide and Chemical Pollutants 2735.1 Mass Spectrometry Data of 1200 Pesticides and ChemicalPollutants Determined by GC-MS, GC-MS-MS, and LC-MS-MS 2775.1.1 Retention Times, Quantifier and Qualifier Ions of567 Pesticides and Chemical Pollutants Determined by GC-MS 2775.1.2 Monitoring of Selected Ions for 567 Pesticidesand Chemical Pollutants Determined by GC-MS 3115.1.3 Retention Time, Quantifier and Qualifier Ions, andCollision Energies of 454 Pesticides and Chemical Pollutants Determined by GC-MS-MS 3215.1.4 Monitoring of Selected Ions for 454 Pesticidesand Chemical Pollutants Determined by GC-MS-MS 3495.1.5 Retention Time, Quantifier and Qualifier Ions,and Collision Energies of 284 Environmental Pollutants by GC-MS-MS 3565.1.6 Retention Times, Selective Ions, and Relative Abundancesof Endosulfans Determined by GC-NCI-MS 3745.1.7 Retention Times, Quantifying and Qualifying Ions,Declustering Potentials, and Collision Energies of 9 Environmental Pollutants Determined by LC-MS-MS 3755.1.8 Retention Times, Quantifying and Qualifying Ions,Fragmentor, and Collision Energies of 569 Pesticidesand Chemical Pollutants Determined by LC-MS-MS 3765.1.9 Accurate Masses, Retention Times, Parent Ions,and Collision Energies of 492 Pesticides and ChemicalPollutants Determined by LC-TOF-MS 4105.2 Linear Equation Parameters of 1200 Pesticides andChemical Pollutants Determined by GC-MS, GC-MS-MS,and LC-MS-MS 4575.2.1 Linear Equations, Linear Ranges, and CorrelationCoefficients of 567 Pesticides and Chemical Pollutants Determined by GC-MS 4575.2.2 Linear Equations, Linear Ranges, and CorrelationCoefficients of 466 Pesticides and Chemical Pollutants Determined by GC-MS-MS 4915.2.3 Linear Equations, Linear Ranges, and CorrelationCoefficients of 284 Environmental Pollutants Determined by GC-MS-MS 5195.2.4 Linear Equations, Linear Ranges, and CorrelationCoefficients of Endosulfans Determined by GC-MS(NCI) 5365.2.5 Linear Equations, Linear Ranges, and CorrelationCoefficients of 9 Environmental Pollutants Determined by LC-MS-MS 5375.2.6 Linear Equations, Linear Ranges, and CorrelationCoefficients of 569 Pesticides and Chemical Pollutants Determined by LC-MS-MS 5385.3 GPC Analytical Parameters of Pesticides and Chemical Pollutants 5725.3.1 GPC Analytical Parameters of 744 Pesticides and Chemical Pollutants 5725.3.2 GPC Analytical Parameters of 107 Pesticides and Chemical Pollutants 599Appendix A: Index of 1039 Pesticides and Chemical Pollutants Determinedby GC-MS, GC-MS-MS and LC-MS-MS 603Appendix B: Solvent Selected and Concentration of Mixed StandardSolution of Pesticides and Chemical Pollutants 661Appendix C: Physicochemical Properties of 900 Pesticidesand Chemical Pollutants 707Appendix D: MRM Chromatograms of 493 Pesticidesand Related Chemicals 791Index 857

封面

书名:农药(第1卷)/农药兽药多组分残留质谱分析技术

作者:庞国芳 著

页数:861

定价:¥788.0

出版社:化学工业出版社

出版日期:2018-01-01

ISBN:9787122349187

PDF电子书大小:114MB 高清扫描完整版