农药兽药多组分残留质谱分析技术:第2卷:Volume Ⅱ:兽药:Veterinary drugs

本书特色

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本书是《农药兽药多组分残留质谱分析技术》的第2卷兽药篇,介绍了65项适用于动物组织(肌肉、肝脏、肾脏和脂肪)、乳制品(牛奶和奶粉)、蜂产品(蜂蜜、蜂王浆及冻干粉)、水产品(河豚鱼、鳗鱼和烤鳗)及动物尿液中20类兽药残留LC-MS/MS分析方法。方法灵敏度和准确度高,可满足欧盟、日本、国际食品法典委员会(CAC)和美国等限量要求。各章按兽药类别,分别介绍了磺胺类、β-受体激动剂类、氨基糖苷类、氯霉素类、β-内酰胺类、大环内酯类和林可胺类、硝基呋喃类代谢物、甾体类同化激素、非甾类同化激素类、糖皮质激素类、氟喹诺酮类、四环素类、镇静剂类、吡唑酮类、喹 啉类、硝基咪唑类、苯并咪唑类、咪唑并噻唑类、硫脲嘧啶类、聚醚类等20类兽药的前处理技术和测定方法,并介绍了兽药的理化性质、代谢和毒理及*残留限量等。本书可供从事食品安全、农业环境保护及农药开发利用等技术研究与应用的技术人员参考,也可作为大学教学参考用书。

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内容简介

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本书是与Elsevier合作出版项目,书中详细介绍了65项适用于动物组织(肌肉、肝脏、肾脏和脂肪)、乳制品(牛奶和奶粉)、蜂产品(蜂蜜、蜂王浆及冻干粉)、水产品(河豚鱼、鳗鱼和烤熳)及动物尿液中20类兽药残留LC-MS/MS分析方法,具有检测限低、回收率高、相对标准偏差低等特点,可满足国际食品法典委员会、欧盟、日本和美国等限量要求。作者庞国芳院士是农药及化学污染物残留分析领域的国际知名专家。

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作者简介

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庞国芳,中国检验检疫科学研究院,研究员,中国工程院院士,国家质检总局首席研究员、国际公职化学家联合会(AOAC)专家,国际AOAC 2014年度 Harvey W. Wiley 奖获得者。近30年一直工作在食品检验检疫一线,致力于食品科学检测技术理论与实践的研究,解决了我国相关出口食品、农产品等遭遇的技术瓶颈,为推动我国对外贸易发展做出了杰出贡献。研究制定了141项国际、国家检测技术标准。在国内、国际出版食品安全检测技术论著10部。发表论文100余篇,35篇被SCI收录。3次荣获国家科学技术进步二等奖,6次荣获国际AOAC组织颁发的科学技术奖励。

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目录

Main Researchers/Editors xxviiPreface xxixBrief Introduction xxxi1. Sulfonamides 11.1 Curative Effects and Side Effects of Sulfonamides 11.2 Chemical Structures and Maximum Residue Limits for Sulfonamide Drugs 21.3 Determination of 16 Sulfonamide Residues in Livestock and Poultry Muscles—LC-MS-MS Method (GB/T 20759-2006) 81.3.1 Scope 81.3.2 Principle 81.3.3 Reagents and Materials 81.3.4 Apparatus 91.3.5 Sample Pretreatment 91.3.6 Determination 91.3.7 Precision 101.3.8 Recovery 12Researchers 12Further Reading 161.4 Determination of 16 Sulfonamide Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22966-2008) 161.4.1 Scope 161.4.2 Principle 161.4.3 Reagents and Materials 171.4.4 Apparatus 171.4.5 Sample Pretreatment 181.4.6 Determination 181.4.7 Precision 191.4.8 Recovery 28Researchers 281.5 Determination of 18 Sulfonamide Residues in Fugu and Eel—LC-MS-MS Method (GB/T 22951-2008) 291.5.1 Scope 291.5.2 Principle 291.5.3 Reagents and Materials 291.5.4 Apparatus 301.5.5 Sample Pretreatment 311.5.6 Determination 311.5.7 Precision 351.5.8 Recovery 36Researchers 401.6 Determination of 8 Sulfonamides residues in Honey—LC-FLD Method (GB/T 18932.5-2002) 411.6.1 Scope 411.6.2 Principle 411.6.3 Reagents and Materials 411.6.4 Apparatus 421.6.5 Sample Pretreatment 421.6.6 Determination 431.6.7 Precision 431.6.8 Recovery 46Researchers 47Further Reading 471.7 Determination of 16 Sulfonamide Residues in Honey—LC-MS-MS Method (GB/T 18932.17-2003) 471.7.1 Scope 471.7.2 Principle 471.7.3 Reagents and Materials 481.7.4 Apparatus 481.7.5 Sample Pretreatment 481.7.6 Determination 491.7.7 Precision 521.7.8 Recovery 52Researchers 55Further Reading 551.8 Determination of 18 Sulfonamide Residues in Royal Jelly—LC-MS-MS Method (GB/T 22947-2008) 561.8.1 Scope 561.8.2 Principle 561.8.3 Reagents and Materials 561.8.4 Apparatus 571.8.5 Sample Pretreatment 581.8.6 Determination 581.8.7 Precision 621.8.8 Recovery 64Researchers 662. β-Adrenoceptor Agonists 672.1 Determination of 12 β-Agonist Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22965-2008) 672.1.1 Scope 672.1.2 Principle 672.1.3 Reagents and Materials 682.1.4 Apparatus 692.1.5 Sample Pretreatment 692.1.6 Determination 702.1.7 Precision 762.1.8 Recovery 76Researchers 78Further Reading 782.2 Determination of 12 β-Agonist Residues in Fugu, Eel,and Baked Eel—LC-MS-MS Method (GB/T 22950-2008) 812.2.1 Scope 812.2.2 Principle 812.2.3 Reagents and Materials 812.2.4 Apparatus 822.2.5 Sample Pretreatment 832.2.6 Determination 842.2.7 Precision 852.2.8 Recovery 85Researchers 85Further Reading 883. Aminoglycoside 913.1 Curative Effects and Side Effects of Streptomycin 913.2 Chemical Structures and Maximum Residue Limits for Streptomycin and Dihydrostreptomycin 923.3 Determination of Streptomycin Residues in Honey—LC-FLD (GB/T 18932.3-2002) 933.3.1 Scope 933.3.2 Principle 933.3.3 Reagents and Materials 933.3.4 Apparatus 943.3.5 Sample Pretreatment 953.3.6 Determination 953.3.7 Precision 973.3.8 Recovery 97Researchers 97Further Reading 973.4 Determination of Streptomycin, Dihydrostreptomycin,and Kanamycin Residues in Milk and MilkPowder—LC-MS-MS Method (GB/T 22969-2008) 983.4.1 Scope 983.4.2 Principle 983.4.3 Reagents and Materials 983.4.4 Apparatus 993.4.5 Preparation and Storage of Test Sample 1003.4.6 Determination 1013.4.7 Precision 1043.4.8 Recovery 104Researchers 1053.5 Determination of Streptomycin, Dihydrostreptomycin,and Kanamycin Residues in Fugu and Eel—LC-MS-MS Method (GB/T 22954-2008) 1053.5.1 Scope 1053.5.2 Principle 1063.5.3 Reagents and Materials 1063.5.4 Apparatus 1073.5.5 Sample pretreatment 1073.5.6 Determination 1083.5.7 Precision 1093.5.8 Recovery 110Researchers 1103.6 Determination of Streptomycin, Dihydrostreptomycin,and Kanamycin Residues in Honey—LC-MS-MS Method(GB/T 22995-2008) 1113.6.1 Scope 1113.6.2 Principle 1113.6.3 Reagents and Materials 1113.6.4 Apparatus 1123.6.5 Sample pretreatment 1123.6.6 Determination 1133.6.7 Precision 1143.6.8 Recovery 115Researchers 1153.7 Determination of Streptomycin, Dihydrostreptomycin,and Kanamycin Residues in Royal Jelly—LC-MS-MS Method(GB/T 22945-2008) 1163.7.1 Scope 1163.7.2 Principle 1163.7.3 Reagents and Materials 1163.7.4 Apparatus 1173.7.5 Sample pretreatment 1183.7.6 Determination 1183.7.7 Precision 1193.7.8 Recovery 120Researchers 1214. Chloramphenicol 1234.1 Curative Effect and Side Effects of Chloramphenicol 1234.2 Chemical Structures and Maximum Residue Limits for Chloramphenicol, Thiamphenicol, and Florfenicol 1234.3 Determination of Chloramphenicol, Thiamphenicol, and Florfenicol Residues in Edible Animal Muscles, Liver, and Aquatic Products—LC-MS-MS Method (GB/T 20756-2006) 1254.3.1 Scope 1254.3.2 Principle 1254.3.3 Reagents and Materials 1254.3.4 Apparatus 1264.3.5 Sample pretreatment 1264.3.6 Determination 1274.3.7 Precision 1284.3.8 Recovery 130Researchers 131Further Reading 1314.4 Determination of Chloramphenicol, Thiamphenicol, and Florfenicol Residues in Fugu, Eel, and Baked Eel—LC-MS-MSMethod (GB/T 22959-2008) 1324.4.1 Scope 1324.4.2 Principle 1324.4.3 Reagents 1324.4.4 Apparatus 1334.4.5 Sample Pretreatment 1344.4.6 Determination 1354.4.7 Precision 1374.4.8 Recovery 138Researchers 1385. β-Lactams 1435.1 Curative Effects and Side Effects of Penicillins 1435.2 Chemical Structures and Maximum Residue Limits for Penicillins 1435.3 Determination of Nine Penicillin Residues in Livestock and Poultry Muscles — LC-MS-MS Method(GB/T 20755-2006) 1475.3.1 Scope 1475.3.2 Principle 1475.3.3 Reagents and Materials 1475.3.4 Apparatus 1485.3.5 Sample Pretreatment 1485.3.6 Determination 1485.3.7 Precision 1495.3.8 Recovery 152Researchers 154Further Reading 1545.4 Determination of Nine Penicillin Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22975-2008) 1545.4.1 Scope 1545.4.2 Principle 1545.4.3 Reagents and Materials 1555.4.4 Apparatus and Equipment 1555.4.5 Sample Pretreatment 1565.4.6 Determination 1565.4.7 Precision 1595.4.8 Recovery 161Researchers 1625.5 Determination of Nine Penicillin Residues in Fugu and Eel—LC-MS-MS Method (GB/T 22952-2008) 1635.5.1 Scope 1635.5.2 Principle 1635.5.3 Reagents and Materials 1635.5.4 Apparatus 1645.5.5 Sample Pretreatment 1645.5.6 Determination 1655.5.7 Precision 1685.5.8 Recovery 170Researchers 1705.6 Method for the Determination of Six Penicillin Residues in Honey — LC-MS-MS Method (GB/T 18932.25-2005) 1715.6.1 Scope 1715.6.2 Principle 1715.6.3 Reagents and Materials 1715.6.4 Apparatus 1715.6.5 Sample Pretreatment 1725.6.6 Determination 1725.6.7 Precision 1755.6.8 Recovery 177Researchers 177Further Reading 1775.7 Determination of Cefapirin, Cephalexin, Cefalonium,Cefquinome Residues in Milk and Milk Powder—LC-MS-MSMethod (GB/T 22989-2008) 1775.7.1 Scope 1775.7.2 Principle 1785.7.3 Reagents and Materials 1785.7.4 Apparatus 1795.7.5 Sample Pretreatment 1795.7.6 Determination 1805.7.7 Precision 1825.7.8 Recovery 182Researchers 1845.8 Determination of Cefazolin, Cefapirin, Cephalexin,Cefalonium, Cefquinome Residues in Fugu andEel—LC-MS-MS Method (GB/T 22960-2008) 1845.8.1 Scope 1845.8.2 Principle 1845.8.3 Reagents and Materials 1845.8.4 Apparatus 1855.8.5 Sample Pretreatment 1855.8.6 Determination 1865.8.7 Precision 1875.8.8 Recovery 189Researchers 1895.9 Determination of Cefazolin, Cephapirin, Cephalexin,Cefalonium, Cefquinome Residues in Honey—LC-MS-MSMethod (GB/T 22942-2008) 1895.9.1 Scope 1895.9.2 Principle 1905.9.3 Reagents and Materials 1905.9.4 Apparatus 1905.9.5 Sample Pretreatment 1915.9.6 Determination 1915.9.7 Precision 1925.9.8 Recovery 194Researchers 1946. Macrolides 1956.1 Curative Effects and Side Effects of Avermectins 1956.2 The Kinetics of Avermectins: Disposition and Metabolism 1966.3 Maximum Residue Limits for Avermectins 1966.4 Determination of Avermectin Residues in Bovine Liver andMuscles—LC-MS-MS Method (GB/T 20748-2006) 1986.4.1 Scope 1986.4.2 Principle 1986.4.3 Reagents and Materials 1986.4.4 Apparatus 1996.4.5 Sample Pretreatment 1996.4.6 Determination 1996.4.7 Precision 2016.4.8 Recovery 202Researchers 203Further Reading 2046.5 Curative Effect and Side Effects of Lincomycin,Oleandomycin, Erythromycin, Tilmicosin, Tylosin,Clindamycin, Spiramycin, Kitasamycin and Josamycin 2046.6 Chemical Structures and Maximum Residue Limits for Lincomycin, Oleandomycin, Erythromycin, Tilmicosin,Tylosin, Clindamycin, Spiramycin, Kitasamycin, and Josamycin 2056.7 Determination of 9 Macroide and Lincosamide Residues in Livestock and Poultry Muscles—LC-MS-MS Method(GB/T 20762-2006) 2096.7.1 Scope 2096.7.2 Principle 2096.7.3 Reagents and Materials 2096.7.4 Apparatus 2106.7.5 Sample Pretreatment 2106.7.6 Determination 2116.7.7 Precision 2136.7.8 Recovery 215Researchers 217Further Reading 2176.8 Determination of Ivermectin, Abamectin, Doramectin,and Eprinomectin Residues in Milk andMilk Powder—LC-MS-MS Method (GB/T 22968-2008) 2176.8.1 Scope 2176.8.2 Principle 2176.8.3 Reagents and Materials 2186.8.4 Apparatus 2186.8.5 Sample Pretreatment 2196.8.6 Determination 2196.8.7 Precision 2226.8.8 Recovery 223Researchers 2236.9 Determination of Ivermectin, Abamectin, Doramectin,and Eprinomectin Residues in Fugu, Eel, and BakedEel—LC-MS-MS Method (GB/T 22953-2008) 2256.9.1 Scope 2256.9.2 Principle 2256.9.3 Reagents and Materials 2256.9.4 Apparatus 2266.9.5 Sample Pretreatment 2266.9.6 Determination 2276.9.7 Precision 2286.9.8 Recovery 230Researchers 2326.10 Determination of Spiramycin, Pirlimycin,Oleandomycin,Tilmicosin,Erythromycin,and Tylosin Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22988-2008) 2326.10.1 Scope 2326.10.2 Principle 2326.10.3 Reagents and Materials 2326.10.4 Apparatus 2336.10.5 Sample Preparation 2336.10.6 Determination 2346.10.7 Precision 2366.10.8 Recovery 237Researchers 2386.11 Determination of Lincomycin, Oleandomycin, Erythromycin,Tilmicosin, Tylosin, Spiramycin, Kitasamycin, and Josamycin Residues in Fugu and Eel—LC-MS-MS Method(GB/T 22964-2008) 2406.11.1 Scope 2406.11.2 Principle 2406.11.3 Reagents and Materials 2406.11.4 Apparatus 2426.11.5 Sample Pretreatment 2426.11.6 Determination 2436.11.7 Precision 2476.11.8 Recovery 248Researchers 2496.12 Determination of Lincomycin, Erythromycin, Spiramycin,Tilmicosin, Tylosin, Josamycin, Kitasamycin, Oleandomycin Residues in Honey—LC-MS-MS Method (GB/T 22941-2008) 2496.12.1 Scope 2496.12.2 Principle 2506.12.3 Reagents and Materials 2506.12.4 Apparatus 2516.12.5 Sample Pretreatment 2516.12.6 Determination 2526.12.7 Precision 2546.12.8 Recovery 2556.13 Determination of Lincomycin, Erythromycin, Tilmicosin,Tylosin, Spiramycin, Clindamycin, Kitasamycin, andJosamycin Residues in Royal Jelly and Lyophilized Royal Jelly Powder—LC-MS-MS Method(GB/T 22946-2008) 2576.13.1 Scope 2576.13.2 Principle 2576.13.3 Reagents and Materials 2576.13.4 Apparatus 2586.13.5 Sample Pretreatmen 2586.13.6 Determination 2606.13.7 Precision 2616.13.8 Recovery 263Researchers 2647. Nitrofurans 2657.1 Curative Effects and Side Effects of Nitrofurans 2657.2 Pharmacokinetics of Nitrofurans 2657.3 Determination of Residues of the Metabolites of Nitrofurans in Pork, Beef, Chicken, Porcine Liver, andAquatic Products—LC-MS-MS Method (GB/T 20752-2006) 2677.3.1 Scope 2677.3.2 Principle 2687.3.3 Reagents and Materials 2687.3.4 Apparatus 2697.3.5 Sample Pretreatment 2697.3.6 Determination 2707.3.7 Precision 2737.3.8 Recovery 273Researchers 275Further Reading 2757.4 Determination for the Residues of Furaltadon,Nitrofurazone, Nitrofurantoin, and FurazolidoneMetabolites in Milk and Milk Powder—LC-MS-MS Method (GB/T 22987-2008) 2757.4.1 Scope 2757.4.2 Principle 2757.4.3 Reagents and Materials 2767.4.4 Apparatus 2777.4.5 Sample Pretreatment 2777.4.6 Determination 2787.4.7 Precision 2807.4.8 Recovery 280Researchers 2817.5 Determination of Residues of the Metabolites of Furaltadone,Nitrofurazone, Nitrofurantoin, and Furazolidone in Honey—LC-MS-MS Method (GB/T 18932.24-2005) 2817.5.1 Scope 2817.5.2 Principle 2827.5.3 Apparatus 2827.5.4 Reagents and Materials 2827.5.5 Sample Pretreatment 2837.5.6 Determination 2837.5.7 Precision 2867.5.8 Recovery 287Researchers 288Further Reading 2888. Anabolic Steroids 2898.1 Curative Effects and Side Effects of Trenbolone 2898.2 Metabolites of Trenbolone 2898.3 Chemical Structures and Maximum Residue Limits for α-Trenbolone and β-Trenbolone 2908.4 Determination of α-Trenbolone, β-Trenbolone Residues in Bovine Muscle, Liver, and Kidney—LC-UV and LC-MS-MS Method (GB/T 20760-2006) 2918.4.1 Scope 2918.4.2 Principle 2928.4.3 Reagents and Materials 2928.4.4 Apparatus 2928.4.5 Sample Pretreatment 2928.4.6 Determination 2938.4.7 Precision 2968.4.8 Recovery 296Researchers 298Further Reading 2988.5 Curative Effects and Side Effects of α-Trenbolone,β-Trenbolone, Nortestosterone and Epi-Nortestosterone 2988.6 Chemical Structures and Maximum Residue Limits forα-Trenbolone, β-Trenbolone, Nortestosterone, and Epi-Nortestosterone 2998.7 Determination of α-Trenbolone, β-Trenbolone,Nortestosterone and Epi-Nortestosterone Residuesin Bovine Urine—LC-MS-MS Method (GB/T 20761-2006) 2998.7.1 Scope 2998.7.2 Principle 2998.7.3 Reagents and Materials 3018.7.4 Apparatus 3018.7.5 Sample Pretreatment 3018.7.6 Determination 3028.7.7 Precision 3038.7.8 Recovery 304Researchers 305Further Reading 3058.8 Determination of Melengestrol Acetate, Chlormadinone Acetate, and Megestrol Acetate Residues in Milk andMilk Powder—HPLC-MS-MS Method (GB/T 22973-2008) 3058.8.1 Scope 3058.8.2 Principle 3058.8.3 Reagents and Materials 3068.8.4 Apparatus 3078.8.5 Sample Pretreatment 3078.8.6 Determination 3088.8.7 Precision 3098.8.8 Recovery 312Researchers 3128.9 Determination of α-Trenbolone, β-Trenbolone,Nortestosterone, and Epi-Nortestosterone Residues inMilk and Milk Powder—LC-MS-MS Method(GB/T 22976-2008) 3128.9.1 Scope 3128.9.2 Principle 3138.9.3 Reagents and Materials 3148.9.4 Apparatus 3148.9.5 Sample Pretreatment 3158.9.6 Determination 3168.9.7 Precision 3178.9.8 Recovery 319Researchers 3208.10 Determination of Testosterone, Epi-Testosterone and Progesterone Residues in Bovine Liver andMuscle—LC-MS-MS Method (GB/T 20758-2006) 3218.10.1 Scope 3218.10.2 Principle 3218.10.3 Reagents and Materials 3218.10.4 Apparatus 3228.10.5 Sample Pretreatment 3228.10.6 Determination 3238.10.7 Precision 3268.10.8 Recovery 327Researchers 328Further Reading 3288.11 Method for the Determination of Melengestrol Acetate,Chlormadinone Acetate, and Megestrol AcetateResidues in Bovine and Porcine Fat—LC-UV(GB/T 20753-2006) 3288.11.1 Scope 3288.11.2 Principle 3288.11.3 Reagents and Materials 3288.11.4 Apparatus 3298.11.5 Sample Pretreatment 3308.11.6 Determination 3318.11.7 Precision 3318.11.8 Recovery 333Researchers 3339. Inanabolic Steroids 3359.1 Curative Effects and Side Effects of Zeranol, Zearalanone,Diethylstilbestrol, Hexestrol, and Dienoestrol 3359.2 The Metabolite of Zeranol, Zearalanone, Diethylstilbestrol,Hexestrol, and Dienoestrol 3369.3 Chemical Structures and Maximum Residue Limits for Zeranol, Zearalanone, Diethylstilbestrol, Hexestrol, and Dienoestrol 3369.4 Determination of Zearalanol, Zearalanone, Diethylstilbestrol,Hexestrol, and Dienoestrol Multiresidues in Bovine and Equine Liver, Kidney, and Muscle—LC-MS-MS Method(GB/T 20766-2006) 3399.4.1 Scope 3399.4.2 Principle 3399.4.3 Reagents and Materials 3399.4.4 Apparatus 3409.4.5 Sample Pretreatment 3409.4.6 Determination 3419.4.7 Precision 3439.4.8 Recovery 343Researchers 344Further Reading 3449.5 Determination of Zearalanol, Diethylstilbestrol,Hexestrol and Dienoestrol Multiresidues in BovineUrine—LC-MS-MS Method (GB/T 20767-2006) 3459.5.1 Scope 3459.5.2 Principle 3459.5.3 Reagents and Materials 3459.5.4 Apparatus 3469.5.5 Sample Pretreatment 3469.5.6 Determination 3479.5.7 Precision 3489.5.8 Recovery 349Researchers 349Further Reading 3509.6 Determination of Zearalanol, Zearalanone, Diethylstilbestrol,Hexestrol, and Dienoestrol Multiresidues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22992-2008) 3509.6.1 Scope 350
9.6.2 Principle 3509.6.3 Reagents and Materials 3509.6.4 Apparatus 3519.6.5 Sample Pretreatment 3529.6.6 Determination 3539.6.7 Precision 3539.6.8 Recovery 356Researchers 3579.7 Determination of Zearalanol, Zearalanone,Diethylstilbestrol, Hexestrol, and Dienoestrol Residuesin Fugu, Eel, and Baked Eel—LC-MS-MS Method(GB/T 22963-2008) 3589.7.1 Scope 3589.7.2 Principle 3589.7.3 Reagents and Materials 3589.7.4 Apparatus 3599.7.5 Sample Pretreatment 3609.7.6 Determination 3619.7.7 Precision 3629.7.8 Recovery 362Researchers 36310. Glucocorticoid 36510.1 Determination of Nine Glucocorticoid Residues in Fugu, Eel, and Baked Eel—LC-MS-MS Method(GB/T 22957-2008) 36510.1.1 Scope 36510.1.2 Principle 36510.1.3 Reagents and Materials 36510.1.4 Apparatus 36610.1.5 Sample Pretreatment 36710.1.6 Determination 36710.1.7 Precision 36910.1.8 Recovery 371Researchers 37111. Fluoroquinolone 37511.1 Curative Effects and Side Effects of Quinolones 37511.2 Pharmacokinetics of Quinolones 37611.3 Chemical Structures and Maximum Residue Limits for Quinolones 37611.4 Determination of 15 Quinolone Residues in Eel and Eel Products—LC-MS-MS Method 37611.4.1 Scope 37611.4.2 Principle 38011.4.3 Reagents and Materials 38011.4.4 Apparatus 38011.4.5 Sample Pretreatment 38011.4.6 Determination 38111.4.7 Precision 38411.4.8 Recovery 385Researchers 385References 39111.5 Determination of Enrofloxacin, Danofloxacin,Ciprofloxacin, Sarafloxacin, Orbifloxacin, Difloxacin, andMarbofloxacin in Milk and Milk Powder—LC-MS-MS Method (GB/T 22985-2008) 39111.5.1 Scope 39111.5.2 Principle 39211.5.3 Reagents and Materials 39211.5.4 Apparatus 39311.5.5 Sample Pretreatment 39311.5.6 Determination 39411.5.7 Precision 39511.5.8 Recovery 399Researchers 40011.6 Method for the Determination of 14 QuinoloneResidues in Honey—LC-MS-MS Method (GB/T 20757-2006) 40111.6.1 Scope 40111.6.2 Principle 40111.6.3 Reagents and Materials 40111.6.4 Apparatus 40211.6.5 Sample Pretreatment 40211.6.6 Determination 40311.6.7 Precision 40411.6.8 Recovery 406Researchers 41012. Tetracyclines 41112.1 Curative Effect and Side Effects 41112.2 Chemical Structures and Maximum Residue Limits for Tetracyclines 41112.3 Determination of Oxytetracycline, Tetracycline,Chlortetracycline, and Doxycycline Residues inEdible Animal Muscles—LC-UV Method (GB/T 20764-2006) 41312.3.1 Scope 41312.3.2 Principle 41312.3.3 Reagents and Materials 41312.3.4 Apparatus 41412.3.5 Sample Pretreatment 41412.3.6 Determination 41512.3.7 Precision 41512.3.8 Recovery 417Researchers 418Further Reading 41812.4 Determination of Oxytetracycline, Tetracycline,Chlortetracycline, and Doxycycline Residues in Milkand Milk Powder—HPLC-UV Method (GB/T 22990-2008) 41812.4.1 Scope 41812.4.2 Principle 41812.4.3 Reagents and Materials 41912.4.4 Apparatus 41912.4.5 Sample Pretreatment 42012.4.6 Determination 42012.4.7 Precision 42112.4.8 Recovery 423Researchers 42412.5 Determination of Oxytetracycline, Tetracycline,Chlortetracycline, and Doxycycline Residues inFugu and Eel—HPLC-UV Method (GB/T 22961-2008) 42412.5.1 Scope 42412.5.2 Principle 42412.5.3 Reagents and Materials 42412.5.4 Apparatus 42512.5.5 Sample pretreatment 42612.5.6 Determination 42712.5.7 Precision 42712.5.8 Recovery 429字数限制,仅显示部分目录。

封面

农药兽药多组分残留质谱分析技术:第2卷:Volume Ⅱ:兽药:Veterinary drugs

书名:农药兽药多组分残留质谱分析技术:第2卷:Volume Ⅱ:兽药:Veterinary drugs

作者:庞国芳著

页数:32,623页

定价:¥588.0

出版社:化学工业出版社

出版日期:2019-11-01

ISBN:9787122349194

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